197 | 10 | 7 |
下载次数 | 被引频次 | 阅读次数 |
为提高陶瓷材料表面的硬度和韧性,热压烧结制备了Al2O3–(W,Ti)C/Al2O3–TiC对称型叠层陶瓷材料。研究了该叠层材料的层厚比和层数对材料表层的硬度、断裂韧性的影响。此外,通过压痕裂纹法的测量和有限元计算均可以得到叠层陶瓷材料表面层的残余应力值,两种方法获得的残余应力值符合得很好。通过有限元计算还可以得到叠层陶瓷材料不同层内的残余应力分布特征。对比实验表明:叠层陶瓷材料表面层较之相应单一材料而言,具有更高的硬度和断裂韧性。叠层陶瓷材料中残余压应力的存在,是叠层陶瓷材料表面层具有高硬度、高韧性的原因。而且通过改变叠层材料的层厚比和层数可改变叠层材料残余应力的分布。
Abstract:In order to increase the hardness and toughness of the surface of ceramics,Al2O3–(W,Ti)C/Al2O3–TiC symmetric laminated materials were prepared by hot pressing.The effects of layer thickness ratio and layer number on the hardness and toughness of the surface of laminated ceramic materials were discussed.The residual stresses developed in the ceramic layers were measured by indentation technique.The obtained residual stress values are in good agreement with residual stresses calculated by the finite element method(FEM).The residual stress distribution in the different layers were also assessed by the FEM.Comparison of the FEM analysis with the experimental results shows that both the hardness and toughness of laminated ceramic materials are better than those of simple materials.The compressive residual stresses on the surface of the composite are the main reason for the improved hardness and toughness of laminated ceramic materials.And the residual stresses can be controlled by changing the relative layer thickness ratio and layer number of laminated ceramic materials.
[1]谭炎,杨辉,葛曼珍.层状复合陶瓷制备技术与界面特性[J].陶瓷学报,1997,18(2):113–117.TAN Yan,YANG Hui,GE Manzhen.J Ceram(in Chinese),1997,18(2):113–117.
[2]CLEGG W J,KENDALL K,ALFORD N M.A simple way to make tough ceramics[J].Nature,1990,347(10):445–447.
[3]包亦望,左岩,石新勇,等.有机–无机层合玻璃的热应力分析[J].航空材料学报,1999,19(3):51–56.BAO Yiwang,ZUO Yan,SHI Xinyong,et al.J Aeronaut Mater(in Chinese),1999,19(3):51–56.
[4]钱晓倩,葛曼珍,吴义兵,等.层状复合陶瓷强韧化机制及其优化设计因素[J].无机材料学报,1999,14(4):520–526.QIAN Xiaoqian,GE Manzhen,WU Yibing,et al.J Inorg Mater(in Chinese),1999,14(4):520–526.
[5]CHARTIER T,MERLE D,BESSON J L.Laminar ceramic composites[J].J Eur Ceram Soc,1995,15:101–107.
[6]KOVAR D,THOULESS M.Simple method for determining frictional sliding resistance and frictional energy dissipation in layered ceramics[J].J Am Ceram Soc,1997,80(3):673–679.
[7]丁新更,葛曼珍,杨辉.氧化铝/ZTA强夹层层状复合陶瓷的制备和性能[J].硅酸盐通报,2000,19(1):50–52.DING Genxin,GE Manzhen,YANG Hui.Bull Chin Ceram Soc(in Chinese),2000,19(1):50–52.
[8]董海,张弘韬.测定工程陶瓷已加工表面残余应力的几种方法[J].磨床与磨削,2000,(1):71–74.DONG Hai,ZHANG Hongtao.Grind Mach Grind(in Chinese),2000,(1):71–74.
[9]CHANDRASEKAR S,CHAUDKRI M M.Indentation cracking in soda lime glass and Ni–Zn ferrite under Knoop and conical indenters and residual stress measurements[J].Philos Mag A,1993,67(5):1187–1218.
[10]AHN Y,CHANDRASEKAR S,FARRIS T N.Determination of surface residual stress in machined ceramics using indentation fracture[J].J Manu Sci Eng,1996,118:483–489.
[11]漳立冰,张清纯.PZT材料中内应力分析[J].理化检验–物理分册,1995,31(2):34–35,38.ZHANG Libing,ZHANG Qingchun.Phys Test Chem Anal Part A(Phys Test)(in Chinese),1995,31(2):34–35,38.
[12]PORTU G.DE,MICELE L,PEZZOTTI G.Laminated ceramic struc-tures from oxide systems[J].Compos Part B:Eng,2006,37:556–567.
[13]PETER Z,David J G,GARY L M.Mechanical characterization of Al2O3/ZrO2hybrid laminates[J].J Eur Ceram Soc,1998,5:2025–2034.
基本信息:
DOI:
中图分类号:TQ174.1
引用信息:
[1]员冬玲,邓建新,段振兴.Al_2O_3-(W,Ti)C/Al_2O_3-TiC对称型叠层陶瓷的结构设计和力学性能[J].硅酸盐学报,2008,No.232(08):1148-1152.
基金信息:
国家自然科学基金(50675120);; 山东省科技攻关项目(2006GG2204017)资助项目